Standard Practice for Evaluating Precision for Test Method Standards in the Rubber and Carbon Black Manufacturing Industries

Importancia y uso:

4.1 Tests are conducted using standard test methods to generate test data that are used to make decisions for commercial, technical, and scientific purposes. It follows that the precision of a particular test method is an important quality characteristic or figure of merit for a test method and a decision process.

4.2 An evaluation of the precision of a test method is normally conducted with (1) some selected group of materials as typically used with that method and (2) with a group of volunteer laboratories that have experience with the test method. The evaluation represents an event in time for the test method for these materials and laboratories. Another ITP precision evaluation with somewhat different materials or even with the same materials with the same laboratories at a different time, may generate precision results that differ from the initial ITP.

4.3 Experience as indicated in Refs (1-4)4 and elsewhere has shown that the poor reproducibility among the laboratories of a typical ITP is almost always due to interlaboratory bias. Certain laboratories are always low or high compared to a reference as well as other laboratories in all tests. This usual outcome for many ITPs is addressed in this practice by the use of the three-step robust analysis procedures as described in Section 7.

4.4 Caution is urged in applying precision results of a particular test method to product testing for consumer-producer product acceptance. Product acceptance procedures should be developed on the basis of precision data obtained in special programs that are specific to the commercial products and to the laboratories of the interested parties for this type of testing.

Subcomité:

D11.16

Referida por:

D4569-06R21, D1513-05R23, D0575-91R24, D5289-19A, D0991-89R20, D1509-24, D0573-04R25, D1506-23, D2240-15R21, D8621-25E01, D2084-19A, D1508-23E01, D1514-23, D1512-23, D0624-00R20, C1187-20A, D5964-16R21, D3314-02R25, D0412-16R21, D6915-23, D1619-22, D8016-22, D3900-17R25, D0531-15R19, D6845-22, D7662-15R24, D7724-18R23E01, D6049-03R22, D3493-21, D0813-07R25, D1278-91AR20, D6047-17R21, F1957-24, D5051-06R21E01, D0623-07R19E01, D5230-21E01, D3493-21, D3848-03R22, D3568-03R22, D1510-25, D1509-24, D4482-11R21, D3187-06R21, D8362-21, D6204-19A, D4569-06R21, D6601-19R24, D3849-22, D0945-22, D7605-11R22, D3346-17R22, F1502-23, F0414-21, D3492-24, D3958-23, D1937-23, D1646-19A, D6204-19A, D5376-06R21, D0430-06R25, D0395-18R25, D3191-10R20, D5297-95R23, D4578-22, D7633-13R22, D3403-07R21, D4986-22, D1513-05R23, D4527-18R23, D5666-95R23, D5044-06R21, D1229-03R24, D0945-22, D7558-09R24, D0395-18R25, D6281-23, D8474-23, D3616-95R24, D5668-21, D6556-21, D4936-10R23, D5963-22, D1646-19A, D3189-06R21, D4026-06R25, D5712-15R25, D6739-20R25, D6147-97R20, D2433-25, D0412-16R21, D3492-24, D3188-06R21, D4574-22, D1414-22, D1514-23, D0926-17R22, D7679-16R24, D6556-21, D4571-22, D2240-15R21, D0575-91R24, D7121-05R24, D7772-15R23, D0380-94R20, F1957-24, D3189-06R21, D6284-17R23, D2228-04R19, D5775-95R23, D1510-25, D8363-20, D6499-24, D4934-02R21, D0573-04R25, D2632-15R24, D0750-12R21, D0430-06R25, D2084-19A, D5670-95R23, D3192-09R19, D3184-11R22, D5902-05R23, D4004-06R25, D1511-12R23, D0572-23, D3265-24A, D1508-23E01, D1630-16R21, D5289-19A, D0865-11R25, D0297-21, D4937-96R21, D2137-11R25, D3185-06R21, D0813-07R25, D4075-06R25, D7854-21, D3186-07R21, D0378-24, D6085-97R22, D1993-22, F0421-15R21, D0412-16R21, D1512-23, D1417-16R21, F1957-24, D1917-03R22, D4572-21, D2414-25, D6515-00R23E01, D5774-95R23, D6746-15R20, F1112-06AR18E01, D4571-22, D4573-22, D3190-06R21, D1991-15R23, D0624-00R20, F1806-21, D3484-06R22, D3191-10R20, D5099-08R22, D1618-23, D6370-23, D5289-19A, D6924-03R17, D1519-95R23, D1278-91AR20, D4315-21, D0454-04R19, D1329-16R21, D1506-23, D1053-92AR24, D6124-06R22, D1415-18, D0297-21, D4678-15AR23, D1076-23, D0471-16AR21, D0471-16AR21, D2663-14R25, D0751-19, D6600-00R23, D6281-23, D0471-16AR21, D1415-18

Volúmen:

09.01

Número ICS:

83.060 (Rubber)

Palabras clave:

general precision; interlaboratory test program; ITP; precision; repeatability; reproducibility; special precision;