Standard Test Method for Automatic Particle Counting of Lubricating and Hydraulic Fluids Using Dilution Techniques to Eliminate the Contribution of Water and Interfering Soft Particles by Light Extinction

Importancia y uso:

5.1 This test method is intended for use in analytical laboratories including onsite in-service oil analysis laboratories.

5.2 Hard particles in lubricating or fluid power systems have a detrimental effect on the system as they cause operating components to wear and also accelerate the degradation of the oil. Hard particles in the oil originate from a variety of sources including generation from within an operating fluid system or contamination, which may occur during the storage and handling of new oils or via ingress into an operating fluid system.

5.3 High levels of contaminants can cause filter blockages and hard particles can have a serious impact on the life of pumps, pistons, gears, bearings, and other moving parts by accelerating wear and erosion.

5.4 Particle count results can be used to aid in assessing the capability of the filtration system responsible for cleaning the fluid, determining if off-line recirculating filtration is needed to clean up the fluid system, or aiding in the decision of whether or not a fluid change is required.

5.5 To accurately measure hard particle contamination levels, it is necessary to negate the particle counts contributed by the presence of small levels of free water. This method includes a process by which this can be accomplished using a water-masking diluent technique whereby water droplets of a size below the target level are finely distributed.

5.6 Certain additives or additive by-products that are semi-insoluble or insoluble in oil, namely the polydimethylsiloxane defoamant additive and oxidation by-products, are known to cause light scattering in automatic particle counters, which in turn causes falsely high counts. These and similar materials are commonly termed “soft particles” (see 3.2.4) and are not known to directly increase wear and erosion within an operating system. The contribution of these particles to the particle size cumulative count is negated with this method.

5.7 The use of dilution in this test method counteracts viscosity effects for highly viscous oils that impact the accuracy of automatic optical particle counting results.

Subcomité:

D02.96.05

Referida por:

D6439-23, D6224-23, D4378-24, D4304-22, D7684-11R20, D7720-21, D8579-24, D4174-23

Volúmen:

05.04

Número ICS:

75.100 (Lubricants, industrial oils and related products), 75.120 (Hydraulic fluids)

Palabras clave:

automatic particle counter; diluent; emulsified water; particle contamination; particle counting; soft particles; water-masking;